Information card for entry 7711167

Structure parameters

• Formula: C32 H32 F6 O6 P2 S2
• Calculated formula: C32 H32 F6 O6 P2 S2
• Title of publication: Reactions of A Lewis acidic methylene phosphonium cationic adduct with olefins
• Authors of publication: Miao, linkun; Yeganeh, Amir; Yeung, Jason; Stephan, Douglas W.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 12.8075 ± 0.0011 Å
• b: 19.1511 ± 0.0015 Å
• c: 15.4157 ± 0.001 Å
• α: 90°
• β: 105.509 ± 0.004°
• γ: 90°
• Cell volume: 3643.5 ± 0.5 ų
• Cell temperature: 150.02 K
• Ambient diffraction temperature: 150.02 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1238
• Residual factor for significantly intense reflections: 0.0687
• Weighted residual factors for significantly intense reflections: 0.157
• Weighted residual factors for all reflections included in the refinement: 0.1868
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No