Information card for entry 7711210

Structure parameters

• Formula: C32 H49 B N6 O1.25 S4 Zn
• Calculated formula: C31 H46 B N6 O S4 Zn
• Title of publication: Synthesis and reactivity of a tris(carbene) zinc chloride complex
• Authors of publication: Sherbow, Tobias J.; Li, Keyan; Zakharov, Lev N.; Pluth, Michael D.
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 18.5324 ± 0.0014 Å
• b: 19.6563 ± 0.0015 Å
• c: 41.276 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 15036 ± 1.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1304
• Residual factor for significantly intense reflections: 0.0759
• Weighted residual factors for significantly intense reflections: 0.1827
• Weighted residual factors for all reflections included in the refinement: 0.2145
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No