Information card for entry 7711330
Formula
C80 H102 B2 K N4 O7
Calculated formula
C80 H102 B2 K N4 O7
Title of publication
Synthesis and Isolation of Dinuclear N,C-Chelate Organoboron Compounds Bridged by Neutral, Anionic, and Dianionic 4,4’-Bipyridine via Reductive Coupling of Pyridines
Authors of publication
Li, Hai-Jun; Feng, Rui; Shi, Xianghui; Wei, Junnian; Xi, Zhenfeng
Journal of publication
Dalton Transactions
Year of publication
2022
a
13.8912 ± 0.0004 Å
b
26.8301 ± 0.0007 Å
c
22.9414 ± 0.0006 Å
α
90°
β
107.383 ± 0.003°
γ
90°
Cell volume
8159.8 ± 0.4 Å3
Cell temperature
180 ± 0.1 K
Ambient diffraction temperature
180 ± 0.1 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0632
Residual factor for significantly intense reflections
0.0514
Weighted residual factors for significantly intense reflections
0.1406
Weighted residual factors for all reflections included in the refinement
0.1483
Goodness-of-fit parameter for all reflections included in the refinement
1.036
Diffraction radiation probe
x-ray
Diffraction radiation wavelength
0.71073 Å
Diffraction radiation type
MoKα
Has coordinates
Yes
Has disorder
No
Has Fobs
No
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https://www.crystallography.net/7711330.html