Information card for entry 7711338

Structure parameters

• Formula: C41 H56 Cl2 N P Pd
• Calculated formula: C41 H56 Cl2 N P Pd
• Title of publication: LPdCl2(amine) Complexes Supported by Terphenyl Phosphanes: Applications in Aryl Amination Reactions
• Authors of publication: Santamaría, Nazaret; Velasco, Clara; Marín, Mario; Maya, Celia; Nicasio, M. Carmen
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 9.1723 ± 0.0005 Å
• b: 11.691 ± 0.0008 Å
• c: 18.9911 ± 0.0013 Å
• α: 97.274 ± 0.002°
• β: 97.47 ± 0.002°
• γ: 102.579 ± 0.002°
• Cell volume: 1945.3 ± 0.2 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0507
• Residual factor for significantly intense reflections: 0.0358
• Weighted residual factors for significantly intense reflections: 0.0733
• Weighted residual factors for all reflections included in the refinement: 0.0808
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No