Information card for entry 7711340

Structure parameters

• Formula: C29 H38 Cl4 N O P Pd
• Calculated formula: C29 H38 Cl4 N O P Pd
• Title of publication: LPdCl2(amine) Complexes Supported by Terphenyl Phosphanes: Applications in Aryl Amination Reactions
• Authors of publication: Santamaría, Nazaret; Velasco, Clara; Marín, Mario; Maya, Celia; Nicasio, M. Carmen
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 23.6446 ± 0.0016 Å
• b: 22.859 ± 0.0014 Å
• c: 11.6653 ± 0.0007 Å
• α: 90°
• β: 103.717 ± 0.003°
• γ: 90°
• Cell volume: 6125.2 ± 0.7 ų
• Cell temperature: 173.15 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0909
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.0917
• Weighted residual factors for all reflections included in the refinement: 0.1081
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No