Information card for entry 7711351

Structure parameters

• Chemical name: FVP-455.4
• Formula: C41 H32 B F9 P2 Pd
• Calculated formula: C41 H32 B F9 P2 Pd
• Title of publication: Diazo Compounds and Palladium-Aryl Complexes: Trapping the Elusive Carbene Migratory Insertion Organometallic Products
• Authors of publication: Villalba, Francisco; Albeniz, Ana Carmen
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 10.1431 ± 0.0004 Å
• b: 22.7544 ± 0.0007 Å
• c: 16.9793 ± 0.0005 Å
• α: 90°
• β: 104.335 ± 0.004°
• γ: 90°
• Cell volume: 3796.8 ± 0.2 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0961
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1122
• Weighted residual factors for all reflections included in the refinement: 0.132
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No