Information card for entry 7711768

Structure parameters

• Formula: C177 H180 Cl16 N8 P4 W4
• Calculated formula: C177 H180 Cl16 N8 P4 W4
• Title of publication: N Heterocyclic Carbene and Cyclic (Alkyl)(amino)carbene Complexes of Molybdenum(IV) and Tungsten(IV)
• Authors of publication: Luz, Christian; Glok, Eduard; Horrer, Günther; Radius, Udo
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 10.0173 ± 0.0001 Å
• b: 17.6425 ± 0.0002 Å
• c: 25.2649 ± 0.0003 Å
• α: 69.869 ± 0.001°
• β: 80.72 ± 0.001°
• γ: 81.98 ± 0.001°
• Cell volume: 4120.38 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0825
• Weighted residual factors for all reflections included in the refinement: 0.0849
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No