Information card for entry 7711807

Structure parameters

• Formula: C33 H42 O4 Si W
• Calculated formula: C33 H42 O4 Si W
• Title of publication: Synthesis and structure of a pyridine-stabilized silanone molybdenum complex and its reactions with PMe3 and acetone
• Authors of publication: Muraoka, Takako; Suzuki, Yuzuki; Tsuchimoto, Masato; Trigagema, Gama; Ueno, Keiji; Koyama, Shinji
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 11.3269 ± 0.0017 Å
• b: 20.581 ± 0.003 Å
• c: 13.585 ± 0.002 Å
• α: 90°
• β: 105.485 ± 0.004°
• γ: 90°
• Cell volume: 3052 ± 0.8 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.028
• Residual factor for significantly intense reflections: 0.0232
• Weighted residual factors for significantly intense reflections: 0.0559
• Weighted residual factors for all reflections included in the refinement: 0.0579
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No