Information card for entry 7711809

Structure parameters

• Formula: C36 H55 Mo O3 P Si2
• Calculated formula: C36 H55 Mo O3 P Si2
• Title of publication: Synthesis and structure of a pyridine-stabilized silanone molybdenum complex and its reactions with PMe3 and acetone
• Authors of publication: Muraoka, Takako; Suzuki, Yuzuki; Tsuchimoto, Masato; Trigagema, Gama; Ueno, Keiji; Koyama, Shinji
• Journal of publication: Dalton Transactions
• Year of publication: 2022
• a: 28.053 ± 0.003 Å
• b: 28.053 ± 0.003 Å
• c: 9.461 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7445.5 ± 1.5 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0442
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0855
• Weighted residual factors for all reflections included in the refinement: 0.0887
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No