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Information card for entry 7711856
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Coordinates | 7711856.cif |
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Original paper (by DOI) | HTML |
Formula | C121 H223.5 Cr11 Cu2 F15 N4.5 O44 |
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Calculated formula | C121 H223.5 Cr11 Cu2 F15 N4.5 O44 |
Title of publication | Templating metallocycles with a macrocycle: synthesis, structures and magnetic studies of {Cr<sub>11</sub>M<sub>2</sub>} complexes. |
Authors of publication | Alotaibi, Rajeh; Brookfield, Adam; Fowler, Jonathan M.; Whitehead, George F. S.; Lockyer, Selena J.; Timco, Grigore A.; Collison, David; Schnack, Jürgen; Winpenny, Richard E. P. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2022 |
Journal volume | 52 |
Journal issue | 1 |
Pages of publication | 20 - 23 |
a | 21.8291 ± 0.0005 Å |
b | 29.6847 ± 0.0007 Å |
c | 31.7603 ± 0.0006 Å |
α | 71.668 ± 0.002° |
β | 73.433 ± 0.002° |
γ | 70.962 ± 0.002° |
Cell volume | 18081.2 ± 0.7 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.108 |
Residual factor for significantly intense reflections | 0.0672 |
Weighted residual factors for significantly intense reflections | 0.1643 |
Weighted residual factors for all reflections included in the refinement | 0.1921 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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