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Information card for entry 7711929
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Coordinates | 7711929.cif |
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Original paper (by DOI) | HTML |
Chemical name | [{κP, κC-(i-Pr)2PO-(5-OMe-C6H4}{κN-Et2NH}NiBr] |
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Formula | C17 H31 Br N Ni O2 P |
Calculated formula | C17 H31 Br N Ni O2 P |
Title of publication | Reactivities of cyclonickellated complexes with hydroxylamines: formation of κ<sup>O</sup>-hydroxylamine and κ<sup>N</sup>-imine adducts and a κ<sup>O</sup>, κ<sup>N</sup>-aminoxide derivative. |
Authors of publication | Sarker, Rajib K.; Mangin, Loïc P; Zargarian, Davit |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2023 |
Journal volume | 52 |
Journal issue | 2 |
Pages of publication | 366 - 375 |
a | 11.3886 ± 0.0004 Å |
b | 11.7955 ± 0.0004 Å |
c | 15.524 ± 0.0005 Å |
α | 90° |
β | 92.048 ± 0.002° |
γ | 90° |
Cell volume | 2084.07 ± 0.12 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0526 |
Residual factor for significantly intense reflections | 0.0516 |
Weighted residual factors for significantly intense reflections | 0.1664 |
Weighted residual factors for all reflections included in the refinement | 0.1684 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.115 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.34139 Å |
Diffraction radiation type | GaKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7711929.html
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