Information card for entry 7711929

Structure parameters

• Chemical name: [{κP, κC-(i-Pr)2PO-(5-OMe-C6H4}{κN-Et2NH}NiBr]
• Formula: C17 H31 Br N Ni O2 P
• Calculated formula: C17 H31 Br N Ni O2 P
• Title of publication: Reactivities of cyclonickellated complexes with hydroxylamines: formation of κ^O-hydroxylamine and κ^N-imine adducts and a κ^O, κ^N-aminoxide derivative.
• Authors of publication: Sarker, Rajib K.; Mangin, Loïc P; Zargarian, Davit
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• Journal volume: 52
• Journal issue: 2
• Pages of publication: 366 - 375
• a: 11.3886 ± 0.0004 Å
• b: 11.7955 ± 0.0004 Å
• c: 15.524 ± 0.0005 Å
• α: 90°
• β: 92.048 ± 0.002°
• γ: 90°
• Cell volume: 2084.07 ± 0.12 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0526
• Residual factor for significantly intense reflections: 0.0516
• Weighted residual factors for significantly intense reflections: 0.1664
• Weighted residual factors for all reflections included in the refinement: 0.1684
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No