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Information card for entry 7711976
Preview
Coordinates | 7711976.cif |
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Original paper (by DOI) | HTML |
Formula | C77 H63 B Br Fe N7 O6 |
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Calculated formula | C77 H63 B Br Fe N7 O6 |
Title of publication | A 1,2,3-triazole-derived pincer-type mesoionic carbene complex of iron(II): carbonyl elimination and hydrosilylation of aromatic aldehydes <i>via</i> the concerted reaction with hydrosilane and a base. |
Authors of publication | Matsubara, Kouki; Yamada, Yuji; Iwasaki, Haruka; Ikeda, Hayao; Kanetsugu, Yuki; Kawata, Satoshi; Koga, Yuji |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2023 |
Journal volume | 52 |
Journal issue | 3 |
Pages of publication | 572 - 582 |
a | 26.864 ± 0.007 Å |
b | 15.259 ± 0.004 Å |
c | 17.79 ± 0.004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 7292 ± 3 Å3 |
Cell temperature | 153 K |
Ambient diffraction temperature | 153 K |
Number of distinct elements | 7 |
Space group number | 52 |
Hermann-Mauguin space group symbol | P n n a |
Hall space group symbol | -P 2a 2bc |
Residual factor for all reflections | 0.0847 |
Residual factor for significantly intense reflections | 0.076 |
Weighted residual factors for significantly intense reflections | 0.2012 |
Weighted residual factors for all reflections included in the refinement | 0.2077 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.137 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7711976.html
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