Information card for entry 7712033

Structure parameters

• Formula: C66.5 H50.5 Co3 N3.5 O13.5
• Calculated formula: C66.5 H50.5 Co3 N3.5 O13.5
• Title of publication: Two pillared-layer metal-organic frameworks based on the pinwheel trinuclear carboxylate-clusters of Zn(II) and Co(II): synthesis, crystal structures, magnetic study, and Lewis acid catalysis.
• Authors of publication: Das, Moyna; Jaswal, Vishakha; Bhambri, Himanshi; Das, Prasenjit; Maity, Suvendu; Ghosh, Prasanta; Mandal, Sanjay K.; Sarkar, Madhushree
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• Journal volume: 52
• Journal issue: 5
• Pages of publication: 1449 - 1460
• a: 19.8959 ± 0.0012 Å
• b: 13.9672 ± 0.001 Å
• c: 24.4832 ± 0.0016 Å
• α: 90°
• β: 109.133 ± 0.003°
• γ: 90°
• Cell volume: 6427.8 ± 0.7 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.088
• Weighted residual factors for significantly intense reflections: 0.2633
• Weighted residual factors for all reflections included in the refinement: 0.2767
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No