Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7712090
Preview
Coordinates | 7712090.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C39 H57 O4 V |
---|---|
Calculated formula | C39 H57 O4 V |
Title of publication | Synthesis and molecular structural studies of racemic chiral-at-vanadium(V) complexes using an unsymmetric achiral phenolic bidentate ligand. |
Authors of publication | Nagata, Koichi; Hino, Ayako; Ube, Hitoshi; Sato, Hiroyasu; Shionoya, Mitsuhiko |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2023 |
Journal volume | 52 |
Journal issue | 11 |
Pages of publication | 3295 - 3299 |
a | 11.3936 ± 0.0003 Å |
b | 13.2903 ± 0.0003 Å |
c | 13.406 ± 0.0003 Å |
α | 75.111 ± 0.002° |
β | 69.895 ± 0.002° |
γ | 75.358 ± 0.002° |
Cell volume | 1811.79 ± 0.08 Å3 |
Cell temperature | 93.15 K |
Ambient diffraction temperature | 93.15 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0365 |
Residual factor for significantly intense reflections | 0.0337 |
Weighted residual factors for significantly intense reflections | 0.0905 |
Weighted residual factors for all reflections included in the refinement | 0.0922 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.082 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7712090.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.