Information card for entry 7712136

Structure parameters

• Formula: C84 H84 N4 O4 P4 Rh2
• Calculated formula: C84 H84 N4 O4 P4 Rh2
• Title of publication: C-H activation in bimetallic rhodium complexes to afford N-heterocyclic carbene pincer complexes.
• Authors of publication: Watson, Lachlan J.; Hill, Anthony F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• Journal volume: 52
• Journal issue: 7
• Pages of publication: 2164 - 2174
• a: 26.9934 ± 0.0004 Å
• b: 12.7673 ± 0.0001 Å
• c: 23.3601 ± 0.0004 Å
• α: 90°
• β: 115.376 ± 0.002°
• γ: 90°
• Cell volume: 7273.9 ± 0.2 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0309
• Residual factor for significantly intense reflections: 0.0292
• Weighted residual factors for significantly intense reflections: 0.0757
• Weighted residual factors for all reflections included in the refinement: 0.077
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No