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Information card for entry 7712142
Preview
Coordinates | 7712142.cif |
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Original paper (by DOI) | HTML |
Formula | C36 Cd3 Cu9 K9.05 N36 Nb54 O234 Si3 |
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Calculated formula | C36 Cd3 Cu9 K9.044 N36 Nb54 O234 Si3 |
Title of publication | Cadmium-containing windmill-like heteropolyoxoniobate macrocycle with high yield for catalyzing Knoevenagel condensation. |
Authors of publication | Liu, Zheng-Yi; Ye, Jian-Ping; Li, Yi-Lun; Sun, Yan-Qiong; Li, Xin-Xiong; Sun, Cai; Zheng, Shou-Tian |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2023 |
Journal volume | 52 |
Journal issue | 5 |
Pages of publication | 1193 - 1197 |
a | 25.5734 ± 0.0004 Å |
b | 26.5996 ± 0.0004 Å |
c | 26.713 ± 0.0004 Å |
α | 61.229 ± 0.002° |
β | 78.987 ± 0.001° |
γ | 81.922 ± 0.001° |
Cell volume | 15609.8 ± 0.5 Å3 |
Cell temperature | 99.99 ± 0.1 K |
Ambient diffraction temperature | 99.99 ± 0.1 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0723 |
Residual factor for significantly intense reflections | 0.0653 |
Weighted residual factors for significantly intense reflections | 0.1799 |
Weighted residual factors for all reflections included in the refinement | 0.1861 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.007 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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