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Information card for entry 7712213
Preview
Coordinates | 7712213.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C46 H45 F6 N O6 P4 Pb S2 |
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Calculated formula | C46 H45 F6 N O6 P4 Pb S2 |
SMILES | [Pb]12([P](c3ccccc3)(c3ccccc3)CC[P]1(CC[P]2(c1ccccc1)c1ccccc1)CC[P](c1ccccc1)c1ccccc1)(OS(=O)(=O)C(F)(F)F)OS(=O)(=O)C(F)(F)F.N#CC |
Title of publication | Synthesis, spectroscopic and structural properties of Sn(II) and Pb(II) triflate complexes with soft phosphine and arsine coordination. |
Authors of publication | Cairns, Kelsey R.; King, Rhys P.; Bannister, Robert D.; Levason, William; Reid, Gillian |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2023 |
Journal volume | 52 |
Journal issue | 8 |
Pages of publication | 2293 - 2308 |
a | 16.3354 ± 0.0005 Å |
b | 14.2959 ± 0.0003 Å |
c | 21.6774 ± 0.0005 Å |
α | 90° |
β | 102.94 ± 0.002° |
γ | 90° |
Cell volume | 4933.8 ± 0.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.047 |
Residual factor for significantly intense reflections | 0.0314 |
Weighted residual factors for significantly intense reflections | 0.0515 |
Weighted residual factors for all reflections included in the refinement | 0.0546 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Diffraction radiation X-ray symbol | K-L~3~ |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7712213.html
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