Information card for entry 7712295

Structure parameters

• Formula: C29 H44 Cu3 Gd N3 O26
• Calculated formula: C29 H44 Cu3 Gd N3 O26
• Title of publication: Tetranuclear [Cu₃Ln] complexes derived from a tetraketone-type ligand.
• Authors of publication: Shiga, Takuya; Miyamoto, Haruka; Okamoto, Yukiko; Oshio, Hiroki; Mihara, Nozomi; Nihei, Masayuki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• a: 8.9376 ± 0.0008 Å
• b: 27.147 ± 0.002 Å
• c: 17.9174 ± 0.0016 Å
• α: 90°
• β: 103.291 ± 0.001°
• γ: 90°
• Cell volume: 4230.8 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.1223
• Weighted residual factors for all reflections included in the refinement: 0.1232
• Goodness-of-fit parameter for all reflections included in the refinement: 1.274
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No