Information card for entry 7712298

Structure parameters

• Formula: C65 H47 B Cl3 F20 N O S Si
• Calculated formula: C65 H47 B Cl3 F20 N O S Si
• Title of publication: Imine-stabilized silylium ions: synthesis, structure and application in catalysis
• Authors of publication: Dajnak, Aymeric; Shi, Limiao; Altınbaş Özpınar, Gül; Lenk, Romaric; Saffon-Merceron, Nathalie; Baceiredo, Antoine; Kato, Tsuyoshi; Müller, Thomas; Maerten, Eddy
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• Journal volume: 52
• Journal issue: 10
• Pages of publication: 3052 - 3058
• a: 18.2031 ± 0.001 Å
• b: 24.9358 ± 0.0016 Å
• c: 26.8374 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12181.7 ± 1.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 9
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0944
• Residual factor for significantly intense reflections: 0.0661
• Weighted residual factors for significantly intense reflections: 0.1569
• Weighted residual factors for all reflections included in the refinement: 0.1764
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No