Information card for entry 7712303
| Formula |
C23 H27 Br3 N4 Pd |
| Calculated formula |
C23 H27 Br3 N4 Pd |
| Title of publication |
Versatile halogenation <i>via</i> a C<sub>NHC</sub>^C<sub>sp3</sub> palladacycle intermediate. |
| Authors of publication |
Teng, Qiaoqiao; Liu, Ziwei; Song, Haobin; Liu, Jiayu; Zhao, Yaru; Jiang, Weihua; Huynh, Han Vinh; Meng, Qi |
| Journal of publication |
Dalton transactions (Cambridge, England : 2003) |
| Year of publication |
2023 |
| Journal volume |
52 |
| Journal issue |
8 |
| Pages of publication |
2223 - 2226 |
| a |
10.6138 ± 0.0006 Å |
| b |
13.7132 ± 0.0009 Å |
| c |
17.3306 ± 0.0011 Å |
| α |
90° |
| β |
97.572 ± 0.002° |
| γ |
90° |
| Cell volume |
2500.5 ± 0.3 Å3 |
| Cell temperature |
170 K |
| Ambient diffraction temperature |
170 K |
| Number of distinct elements |
5 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/c 1 |
| Hall space group symbol |
-P 2ybc |
| Residual factor for all reflections |
0.1408 |
| Residual factor for significantly intense reflections |
0.0821 |
| Weighted residual factors for significantly intense reflections |
0.1548 |
| Weighted residual factors for all reflections included in the refinement |
0.1747 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.066 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/7712303.html
