Crystallography Open Database

Information card for entry 7712366

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Coordinates	7712366.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H39 B2 Br P2
Calculated formula	C16 H39 B2 Br P2
Title of publication	Reactivity of triphosphinoboranes towards H3B∙SMe2: Access to derivatives of boraphosphacycloalkanes with diversified substituents
Authors of publication	Ordyszewska, Anna; Chojnacki, Jarosław; Grubba, Rafał
Journal of publication	Dalton Transactions
Year of publication	2023
a	8.5887 ± 0.0009 Å
b	13.8357 ± 0.0016 Å
c	9.1332 ± 0.0011 Å
α	90°
β	98.207 ± 0.009°
γ	90°
Cell volume	1074.2 ± 0.2 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.045
Residual factor for significantly intense reflections	0.0343
Weighted residual factors for significantly intense reflections	0.0746
Weighted residual factors for all reflections included in the refinement	0.079
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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