Crystallography Open Database

Information card for entry 7712368

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Coordinates	7712368.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H64 B3 P3
Calculated formula	C28 H64 B3 P3
Title of publication	Reactivity of triphosphinoboranes towards H3B∙SMe2: Access to derivatives of boraphosphacycloalkanes with diversified substituents
Authors of publication	Ordyszewska, Anna; Chojnacki, Jarosław; Grubba, Rafał
Journal of publication	Dalton Transactions
Year of publication	2023
a	11.0382 ± 0.0002 Å
b	19.0404 ± 0.0003 Å
c	15.9387 ± 0.0003 Å
α	90°
β	106.256 ± 0.002°
γ	90°
Cell volume	3215.94 ± 0.1 Å³
Cell temperature	120 K
Ambient diffraction temperature	120 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0523
Residual factor for significantly intense reflections	0.0388
Weighted residual factors for significantly intense reflections	0.0969
Weighted residual factors for all reflections included in the refinement	0.1027
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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