Information card for entry 7712492

Structure parameters

• Formula: C54 H51 Al Cl2 F2 N2 O
• Calculated formula: C54 H51 Al Cl2 F2 N2 O
• Title of publication: Synthesis, Characterisation and Reactivity studies of Chiral β-Diketiminate-like Supported Aluminium Lewis Acid Complexes Towards Difficult Diels Alder Cycloadditions
• Authors of publication: Dissanayake, Deepamali; Forsyth, Craig M.; Vidovic, Dragoslav
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 10.0591 ± 0.0001 Å
• b: 10.2551 ± 0.0002 Å
• c: 12.5367 ± 0.0002 Å
• α: 113.677 ± 0.002°
• β: 95.189 ± 0.001°
• γ: 102.207 ± 0.001°
• Cell volume: 1135.18 ± 0.04 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0793
• Weighted residual factors for all reflections included in the refinement: 0.0799
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No