Information card for entry 7712841

Structure parameters

• Chemical name: 5
• Formula: C28 H64 Fe Si9
• Calculated formula: C28 H64 Fe Si9
• Title of publication: Persilylation of Ferrocene: The Ultimate Discipline in Sterically Overcrowded Metal Complexes
• Authors of publication: Rupf, Susanne M.; Sievers, Robin; Riemann, Paulin S.; Reimann, Marc; Kaupp, Martin; Fasting, Dr. Carlo; Malischewski, Moritz
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 11.9336 ± 0.0007 Å
• b: 18.9321 ± 0.0012 Å
• c: 20.4215 ± 0.0013 Å
• α: 63.84 ± 0.002°
• β: 77.549 ± 0.002°
• γ: 88.306 ± 0.002°
• Cell volume: 4032.5 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0534
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.1001
• Weighted residual factors for all reflections included in the refinement: 0.1055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No