Information card for entry 7712944

Structure parameters

• Formula: C24 H30 N2 O6 Si
• Calculated formula: C24 H30 N2 O6 Si
• Title of publication: Quantitative Raman microscopy to describe structural organisation in hollow microcrystals built from silicon catecholate and amines
• Authors of publication: Volkov, Victor V.; Blundell, Toby J.; Argent, Stephen; Perry, Carole Celia
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 12.3695 ± 0.0002 Å
• b: 21.4394 ± 0.0003 Å
• c: 8.5405 ± 0.0001 Å
• α: 90°
• β: 99.442 ± 0.001°
• γ: 90°
• Cell volume: 2234.21 ± 0.05 ų
• Cell temperature: 100.15 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0834
• Residual factor for significantly intense reflections: 0.0792
• Weighted residual factors for significantly intense reflections: 0.2435
• Weighted residual factors for all reflections included in the refinement: 0.2467
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.6889 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No