Information card for entry 7713042

Structure parameters

• Formula: C39 H23 F34 N2 P3
• Calculated formula: C39 H23 F34 N2 P3
• Title of publication: Anionic N-Heterocyclic Carbenes Featuring Weakly Coordinating Perfluoroalkylphosphorane Moieties
• Authors of publication: Zapf, Ludwig; Radius, Udo; Finze, Maik
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 20.4078 ± 0.0002 Å
• b: 14.2097 ± 0.0001 Å
• c: 15.9722 ± 0.0001 Å
• α: 90°
• β: 96.907 ± 0.001°
• γ: 90°
• Cell volume: 4598.14 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 0.3 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0315
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for significantly intense reflections: 0.0787
• Weighted residual factors for all reflections included in the refinement: 0.0794
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No