Information card for entry 7713287

Structure parameters

• Formula: C60 H68 O16 S2 Si8
• Calculated formula: C60 H68 O16 S2 Si8
• Title of publication: Synthesis and Characterization of Sulfide/Sulfone-Containing 18-8-18-Membered-Ring Ladder-Type Siloxanes
• Authors of publication: Zheng, Zhan-Jiang; Liu, Yujia; Takeda, Nobuhiro; Unno, Masafumi
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 21.122 ± 0.003 Å
• b: 10.678 ± 0.0018 Å
• c: 29.541 ± 0.005 Å
• α: 90°
• β: 94.396 ± 0.004°
• γ: 90°
• Cell volume: 6643.1 ± 1.8 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0346
• Residual factor for significantly intense reflections: 0.0296
• Weighted residual factors for significantly intense reflections: 0.0786
• Weighted residual factors for all reflections included in the refinement: 0.0833
• Goodness-of-fit parameter for all reflections included in the refinement: 1.096
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No