Homoleptic complexes of isocyano- and diisocyanobiazulenes with a 12-electron, ligand-based redox capacity
Authors of publication
Connelly, Patrick T.; Applegate, Jason C.; Maldonado, David A.; Okeowo, Monisola K.; Henke, Wade C.; Oliver, Allen Grayson; Berrie, Cindy L.; Barybin, Mikhail V.
Journal of publication
Dalton Transactions
Year of publication
2023
a
10.7018 ± 0.0005 Å
b
16.7383 ± 0.0009 Å
c
20.6013 ± 0.0011 Å
α
90.327 ± 0.002°
β
92.499 ± 0.002°
γ
91.085 ± 0.002°
Cell volume
3686.1 ± 0.3 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0728
Residual factor for significantly intense reflections
0.0503
Weighted residual factors for significantly intense reflections
0.1292
Weighted residual factors for all reflections included in the refinement
0.1414
Goodness-of-fit parameter for all reflections included in the refinement
