Information card for entry 7713712

Structure parameters

• Formula: C18 H35 Al Cl N2 P Si
• Calculated formula: C18 H35 Al Cl N2 P Si
• Title of publication: Synthesis and reactivity of alkali metal aluminates bearing bis(organoamido)phosphane ligand
• Authors of publication: Vrána, Jan; Ruzickova, Zdenka; R°užička, Aleš; Dostál, Libor
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 18.447 ± 0.0011 Å
• b: 12 ± 0.0017 Å
• c: 27.745 ± 0.0008 Å
• α: 90°
• β: 131.264 ± 0.007°
• γ: 90°
• Cell volume: 4616.6 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0531
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for significantly intense reflections: 0.0871
• Weighted residual factors for all reflections included in the refinement: 0.1011
• Goodness-of-fit parameter for all reflections included in the refinement: 1.116
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No