Information card for entry 7714040

Structure parameters

• Formula: C35 H65 Fe Si8
• Calculated formula: C35 H65 Fe Si8
• Title of publication: Four- and Three-coordinate Planar Iron(II) Complexes Supported by Bulky Organosilyl Ligands
• Authors of publication: Ishii, Reon; Nakagawa, Minesato; Wada, Yoshimasa; Sunada, Yusuke
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 9.4785 ± 0.0007 Å
• b: 23.6413 ± 0.0017 Å
• c: 21.2483 ± 0.0016 Å
• α: 90°
• β: 102.331 ± 0.007°
• γ: 90°
• Cell volume: 4651.6 ± 0.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0366
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0833
• Weighted residual factors for all reflections included in the refinement: 0.0863
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.4122 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No