Information card for entry 7714049

Structure parameters

• Formula: C45 H70 K N5 Si11
• Calculated formula: C45 H70 K N5 Si11
• Title of publication: Synthesis and Functionalization of the Six-Vertex Anionic Amido-Substituted Silicon Cluster [Si6{N(SiMe3)Ph}5]−
• Authors of publication: Lips, Felicitas; Helmer, Joschua; Hepp, Alexander; Berger, Raphael J. F.
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 15.5664 ± 0.0005 Å
• b: 18.725 ± 0.0006 Å
• c: 19.2084 ± 0.0006 Å
• α: 90°
• β: 100.86 ± 0.002°
• γ: 90°
• Cell volume: 5498.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0807
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1439
• Weighted residual factors for all reflections included in the refinement: 0.1621
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No