Information card for entry 7714051

Structure parameters

• Formula: C51 H76 Cl5 N5 Si12
• Calculated formula: C51 H76 Cl5 N5 Si12
• Title of publication: Synthesis and Functionalization of the Six-Vertex Anionic Amido-Substituted Silicon Cluster [Si6{N(SiMe3)Ph}5]−
• Authors of publication: Lips, Felicitas; Helmer, Joschua; Hepp, Alexander; Berger, Raphael J. F.
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 13.0493 ± 0.0005 Å
• b: 13.4471 ± 0.0006 Å
• c: 20.7283 ± 0.0009 Å
• α: 71.982 ± 0.002°
• β: 84.352 ± 0.002°
• γ: 72.014 ± 0.001°
• Cell volume: 3289.9 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0284
• Residual factor for significantly intense reflections: 0.0269
• Weighted residual factors for significantly intense reflections: 0.0756
• Weighted residual factors for all reflections included in the refinement: 0.0765
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No