Information card for entry 7714094

Structure parameters

• Formula: C17 H25 N2 P
• Calculated formula: C17 H25 N2 P
• Title of publication: Triphosphiranes as Phosphinidene-Transfer Agents – Synthesis of Regular and Chelating NHC Phosphinidene Adducts
• Authors of publication: Siewert, Jan-Erik; Schumann, André; Wellnitz, Tim; Dankert, Fabian; Hering-Junghans, Christian
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 8.0396 ± 0.0002 Å
• b: 15.6897 ± 0.0004 Å
• c: 58.4856 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7377.3 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0849
• Residual factor for significantly intense reflections: 0.0761
• Weighted residual factors for significantly intense reflections: 0.1771
• Weighted residual factors for all reflections included in the refinement: 0.1811
• Goodness-of-fit parameter for all reflections included in the refinement: 1.199
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No