Crystallography Open Database

Information card for entry 7714097

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Coordinates	7714097.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H31 N2 P
Calculated formula	C20 H31 N2 P
Title of publication	Triphosphiranes as Phosphinidene-Transfer Agents – Synthesis of Regular and Chelating NHC Phosphinidene Adducts
Authors of publication	Siewert, Jan-Erik; Schumann, André; Wellnitz, Tim; Dankert, Fabian; Hering-Junghans, Christian
Journal of publication	Dalton Transactions
Year of publication	2023
a	31.2584 ± 0.0009 Å
b	8.8082 ± 0.0002 Å
c	14.9274 ± 0.0004 Å
α	90°
β	107.128 ± 0.001°
γ	90°
Cell volume	3927.68 ± 0.18 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0473
Residual factor for significantly intense reflections	0.0381
Weighted residual factors for significantly intense reflections	0.0994
Weighted residual factors for all reflections included in the refinement	0.1083
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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