Information card for entry 7714105

Structure parameters

• Formula: C37 H46 Cl6 Ge2 N4 P2
• Calculated formula: C36 H44 Cl4 Ge2 N4 P2
• Title of publication: Triphosphiranes as Phosphinidene-Transfer Agents – Synthesis of Regular and Chelating NHC Phosphinidene Adducts
• Authors of publication: Siewert, Jan-Erik; Schumann, André; Wellnitz, Tim; Dankert, Fabian; Hering-Junghans, Christian
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 8.7735 ± 0.0007 Å
• b: 15.3647 ± 0.0012 Å
• c: 16.7707 ± 0.0013 Å
• α: 76.373 ± 0.003°
• β: 89.218 ± 0.003°
• γ: 83.018 ± 0.002°
• Cell volume: 2180.5 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0278
• Residual factor for significantly intense reflections: 0.0263
• Weighted residual factors for significantly intense reflections: 0.0672
• Weighted residual factors for all reflections included in the refinement: 0.0684
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No