Information card for entry 7714107

Structure parameters

• Formula: C26 H43 N2 P
• Calculated formula: C26 H43 N2 P
• Title of publication: Triphosphiranes as Phosphinidene-Transfer Agents – Synthesis of Regular and Chelating NHC Phosphinidene Adducts
• Authors of publication: Siewert, Jan-Erik; Schumann, André; Wellnitz, Tim; Dankert, Fabian; Hering-Junghans, Christian
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 16.679 ± 0.002 Å
• b: 17.697 ± 0.002 Å
• c: 18.581 ± 0.003 Å
• α: 89.3374 ± 0.0023°
• β: 73.1646 ± 0.0021°
• γ: 78.0995 ± 0.0022°
• Cell volume: 5129.8 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1212
• Residual factor for significantly intense reflections: 0.0578
• Weighted residual factors for significantly intense reflections: 0.1201
• Weighted residual factors for all reflections included in the refinement: 0.1499
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No