Information card for entry 7714121

Structure parameters

• Formula: C18 H39 Ge Mn P4
• Calculated formula: C18 H39 Ge Mn P4
• Title of publication: Reactions of [(dmpe)₂MnH(C₂H₄)] with hydrogermanes to form germylene, germyl, hydrogermane, and germanide complexes.
• Authors of publication: Price, Jeffrey S.; Vargas-Baca, Ignacio; Emslie, David J. H.; Britten, James F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• a: 8.9471 ± 0.0017 Å
• b: 16.251 ± 0.008 Å
• c: 16.702 ± 0.004 Å
• α: 90°
• β: 96.35 ± 0.02°
• γ: 90°
• Cell volume: 2413.6 ± 1.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0705
• Weighted residual factors for all reflections included in the refinement: 0.0742
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No