Information card for entry 7714158

Structure parameters

• Formula: C23 H30.7 Cl Fe N2 O0.35 P Pd
• Calculated formula: C23 H30.707 Cl Fe N2 O0.3535 P Pd
• Title of publication: Synthesis and reactivity of Pd(II) imidoyl complexes obtained by insertion of isocyanoferrocene into the Pd-C bonds of orthopalladated precursors
• Authors of publication: Franc, Michal; Vosahlo, Petr; Schulz, Jiří; Cisarova, Ivana; Štěpnička, Petr
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 10.3488 ± 0.0005 Å
• b: 13.782 ± 0.0007 Å
• c: 17.1619 ± 0.0009 Å
• α: 101.004 ± 0.002°
• β: 95.44 ± 0.002°
• γ: 96.566 ± 0.002°
• Cell volume: 2369.9 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0225
• Residual factor for significantly intense reflections: 0.0208
• Weighted residual factors for significantly intense reflections: 0.05
• Weighted residual factors for all reflections included in the refinement: 0.051
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No