Information card for entry 7714287

Structure parameters

• Formula: C72 H69 O6 Pr Si3
• Calculated formula: C72 H69 O6 Pr Si3
• Title of publication: Tripodal tris(siloxide) Ligand Supported Trivalent Rare-earth Metal Complexes and Redox Reactivity
• Authors of publication: Guo, Hui; Hong, Dongjing; Cui, Peng
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 14.894 ± 0.003 Å
• b: 30.171 ± 0.006 Å
• c: 18.312 ± 0.003 Å
• α: 90°
• β: 102.716 ± 0.003°
• γ: 90°
• Cell volume: 8027 ± 3 ų
• Cell temperature: 300 K
• Ambient diffraction temperature: 300 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1555
• Residual factor for significantly intense reflections: 0.0792
• Weighted residual factors for significantly intense reflections: 0.1795
• Weighted residual factors for all reflections included in the refinement: 0.2132
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No