Information card for entry 7714289

Structure parameters

• Formula: C68 H61 Ce Cl O5 Si3
• Calculated formula: C68 H61 Ce Cl O5 Si3
• Title of publication: Tripodal tris(siloxide) Ligand Supported Trivalent Rare-earth Metal Complexes and Redox Reactivity
• Authors of publication: Guo, Hui; Hong, Dongjing; Cui, Peng
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 13.824 ± 0.002 Å
• b: 14.321 ± 0.002 Å
• c: 19.077 ± 0.003 Å
• α: 97.802 ± 0.002°
• β: 101.973 ± 0.002°
• γ: 116.853 ± 0.002°
• Cell volume: 3180.2 ± 0.8 ų
• Cell temperature: 300 K
• Ambient diffraction temperature: 300 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1805
• Residual factor for significantly intense reflections: 0.075
• Weighted residual factors for significantly intense reflections: 0.1485
• Weighted residual factors for all reflections included in the refinement: 0.1903
• Goodness-of-fit parameter for all reflections included in the refinement: 0.958
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No