Information card for entry 7714292

Structure parameters

• Formula: C72 H69 O6 Si3 Tb
• Calculated formula: C72 H69 O6 Si3 Tb
• Title of publication: Tripodal tris(siloxide) Ligand Supported Trivalent Rare-earth Metal Complexes and Redox Reactivity
• Authors of publication: Guo, Hui; Hong, Dongjing; Cui, Peng
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 13.9197 ± 0.0004 Å
• b: 18.7147 ± 0.0005 Å
• c: 23.9418 ± 0.0007 Å
• α: 90°
• β: 91.992 ± 0.001°
• γ: 90°
• Cell volume: 6233.1 ± 0.3 ų
• Cell temperature: 300 K
• Ambient diffraction temperature: 300 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0505
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.0708
• Weighted residual factors for all reflections included in the refinement: 0.0807
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No