Information card for entry 7714357

Structure parameters

• Formula: C26 H42 Br4 In Rh
• Calculated formula: C26 H42 Br4 In Rh
• Title of publication: Rhodium complexes with planar-chiral cyclopentadienyl ligands: synthesis from tert-butylacetylene and catalytic performance in C-H activation of arylhydroxamates
• Authors of publication: Kolos, Andrey; Nelyubina, Yulia V.; Podyacheva, Evgeniya; Perekalin, Dmitry S.
• Journal of publication: Dalton Transactions
• Year of publication: 2023
• a: 15.871 ± 0.003 Å
• b: 12.1783 ± 0.0017 Å
• c: 16.655 ± 0.003 Å
• α: 90°
• β: 107.52 ± 0.01°
• γ: 90°
• Cell volume: 3069.8 ± 0.9 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2029
• Residual factor for significantly intense reflections: 0.1583
• Weighted residual factors for significantly intense reflections: 0.3806
• Weighted residual factors for all reflections included in the refinement: 0.4089
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No