Information card for entry 7714465

Structure parameters

• Chemical name: [K(18-c-6)][F-1]
• Formula: C48 H46.78 F49.99 Ge2 K2 O20
• Calculated formula: C48 H46.774 F49.997 Ge2 K2 O20
• Title of publication: A neutral germanium-centred hard and soft lewis superacid and its unique reactivity towards hydrosilanes.
• Authors of publication: Tschernuth, Florian S.; Kostenko, Arseni; Stigler, Sebastian; Gradenegger, Anna; Inoue, Shigeyoshi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• Journal volume: 53
• Journal issue: 1
• Pages of publication: 74 - 81
• a: 11.2001 ± 0.001 Å
• b: 15.7831 ± 0.0014 Å
• c: 22.3057 ± 0.0019 Å
• α: 107.062 ± 0.003°
• β: 102.834 ± 0.003°
• γ: 95.235 ± 0.003°
• Cell volume: 3623.2 ± 0.6 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0451
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0717
• Weighted residual factors for all reflections included in the refinement: 0.0765
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No