Information card for entry 7714506

Structure parameters

• Formula: C68 H58 Cl N7 Ni2 O9
• Calculated formula: C68 H58 Cl N7 Ni2 O9
• Title of publication: Bimetallic nickel complexes containing imidazole-based phenolate ligands as efficient catalysts for the copolymerization of carbon dioxide with epoxides.
• Authors of publication: Hsu, Han-Fang; Liu, Guan-Lin; Su, Yu-Chia; Ko, Bao-Tsan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2023
• Journal volume: 53
• Journal issue: 1
• Pages of publication: 299 - 314
• a: 11.431 ± 0.0014 Å
• b: 13.7228 ± 0.0016 Å
• c: 21.986 ± 0.003 Å
• α: 85.922 ± 0.004°
• β: 74.86 ± 0.005°
• γ: 84.965 ± 0.004°
• Cell volume: 3312.1 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0862
• Residual factor for significantly intense reflections: 0.0659
• Weighted residual factors for significantly intense reflections: 0.1621
• Weighted residual factors for all reflections included in the refinement: 0.1763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No