Information card for entry 7714808

Structure parameters

• Formula: C223 H379 Cl6 F8 N16 Ni24 O80.5
• Calculated formula: C160 H232 F8 N16 Ni24 O80
• Title of publication: Tetracosanuclear nickel complexes as effective catalysts for cycloaddition of carbon dioxide with epoxides.
• Authors of publication: Liu, Guan-Lin; Wu, En-Hsu; Hung, Yu-Ching; Chou, Wei-Chi; Hung, Chia-Hsin; Lin, Chu-Chieh; Ko, Bao-Tsan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 4
• Pages of publication: 1425 - 1429
• a: 24.8794 ± 0.001 Å
• b: 26.4236 ± 0.001 Å
• c: 43.2603 ± 0.0017 Å
• α: 90°
• β: 93.397 ± 0.002°
• γ: 90°
• Cell volume: 28389.5 ± 1.9 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1216
• Residual factor for significantly intense reflections: 0.0832
• Weighted residual factors for significantly intense reflections: 0.213
• Weighted residual factors for all reflections included in the refinement: 0.243
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No