Information card for entry 7714810

Structure parameters

• Formula: C234 H388 Cl116 N16 Ni24 O88
• Calculated formula: C176 H272 N16 Ni24 O88
• Title of publication: Tetracosanuclear nickel complexes as effective catalysts for cycloaddition of carbon dioxide with epoxides.
• Authors of publication: Liu, Guan-Lin; Wu, En-Hsu; Hung, Yu-Ching; Chou, Wei-Chi; Hung, Chia-Hsin; Lin, Chu-Chieh; Ko, Bao-Tsan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 4
• Pages of publication: 1425 - 1429
• a: 24.885 ± 0.0012 Å
• b: 24.885 ± 0.0012 Å
• c: 73.876 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 45749 ± 5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 87
• Hermann-Mauguin space group symbol: I 4/m
• Hall space group symbol: -I 4
• Residual factor for all reflections: 0.0963
• Residual factor for significantly intense reflections: 0.0846
• Weighted residual factors for significantly intense reflections: 0.2303
• Weighted residual factors for all reflections included in the refinement: 0.2375
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No