Crystallography Open Database

Information card for entry 7714863

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Coordinates	7714863.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H74 Fe O Si8
Calculated formula	C28 H74 Fe O Si8
Title of publication	Planar three-coordinate iron(II) complexes supported by sterically demanding -Si(SiMe<sub>3</sub>)<sub>2</sub>(SiMe<sub>2</sub><sup><i>t</i></sup>Bu) ligands.
Authors of publication	Ishii, Reon; Sunada, Yusuke
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	4
Pages of publication	1421 - 1424
a	10.5191 ± 0.0002 Å
b	22.8961 ± 0.0004 Å
c	18.6336 ± 0.0003 Å
α	90°
β	99.1085 ± 0.0019°
γ	90°
Cell volume	4431.24 ± 0.14 Å³
Cell temperature	133 K
Ambient diffraction temperature	133 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0341
Residual factor for significantly intense reflections	0.0295
Weighted residual factors for significantly intense reflections	0.077
Weighted residual factors for all reflections included in the refinement	0.0795
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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