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Information card for entry 7714874
Preview
Coordinates | 7714874.cif |
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Original paper (by DOI) | HTML |
Formula | C26 H43 Br0.28 F4.34 N O3 P2.73 Re |
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Calculated formula | C26 H43 Br0.278 F4.332 N O3 P2.722 Re |
Title of publication | Induced <i>fac</i>-<i>mer</i> rearrangements in {M(CO)<sub>3</sub>}<sup>+</sup> complexes (M = Re, <sup>99(m)</sup>Tc) by a PNP ligand. |
Authors of publication | Besmer, Manuel Luca; Schwitter, Flurina; Battistin, Federica; Braband, Henrik; Fox, Thomas; Spingler, Bernhard; Alberto, Roger |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2024 |
Journal volume | 53 |
Journal issue | 4 |
Pages of publication | 1434 - 1438 |
a | 8.4694 ± 0.0002 Å |
b | 12.7901 ± 0.0002 Å |
c | 15.8962 ± 0.0003 Å |
α | 105.675 ± 0.002° |
β | 104.744 ± 0.002° |
γ | 92.815 ± 0.002° |
Cell volume | 1590.42 ± 0.06 Å3 |
Cell temperature | 159.99 ± 0.1 K |
Ambient diffraction temperature | 159.99 ± 0.1 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0609 |
Residual factor for significantly intense reflections | 0.0558 |
Weighted residual factors for significantly intense reflections | 0.1477 |
Weighted residual factors for all reflections included in the refinement | 0.1523 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.082 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7714874.html
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