Information card for entry 7715247

Structure parameters

• Formula: C82 H102 Si6
• Calculated formula: C61 H81 Si6
• Title of publication: Hexadentate poly-Lewis acids based on the bowl-shaped tribenzotriquinacene.
• Authors of publication: Franke, Maurice; Klingsiek, Maximilian J.; Buth, Julian; Lamm, Jan-Hendrik; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 18
• Pages of publication: 7751 - 7762
• a: 27.3971 ± 0.0004 Å
• b: 25.3293 ± 0.0003 Å
• c: 24.4731 ± 0.0003 Å
• α: 90°
• β: 99.932 ± 0.001°
• γ: 90°
• Cell volume: 16728.6 ± 0.4 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 3
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.1033
• Residual factor for significantly intense reflections: 0.0979
• Weighted residual factors for significantly intense reflections: 0.288
• Weighted residual factors for all reflections included in the refinement: 0.2938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No