Crystallography Open Database

Information card for entry 7715249

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Coordinates	7715249.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C155 H300 Al6 Si24
Calculated formula	C127 H268 Al6 Si24
Title of publication	Hexadentate poly-Lewis acids based on the bowl-shaped tribenzotriquinacene.
Authors of publication	Franke, Maurice; Klingsiek, Maximilian J.; Buth, Julian; Lamm, Jan-Hendrik; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	18
Pages of publication	7751 - 7762
a	39.1993 ± 0.0006 Å
b	22.8491 ± 0.0002 Å
c	46.9723 ± 0.0007 Å
α	90°
β	109.481 ± 0.0016°
γ	90°
Cell volume	39663.2 ± 1 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0808
Residual factor for significantly intense reflections	0.0705
Weighted residual factors for significantly intense reflections	0.1877
Weighted residual factors for all reflections included in the refinement	0.1972
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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